乳业科学与技术 ›› 0, Vol. ›› Issue (): 0-0.

• 基础研究 •    下一篇

牦牛酥油微囊粉的理化性质和结构特性表征

王茜1,罗毅皓2,孙万成1   

  1. 1. 青海大学农牧学院
    2. 青海大学
  • 收稿日期:2024-12-06 修回日期:2025-02-08 出版日期:2025-01-01 发布日期:2025-02-28
  • 通讯作者: 王茜

Physicochemical properties and structural characteristics of yak butter microencapsulated powders

茜 王, ,   

  • Received:2024-12-06 Revised:2025-02-08 Published:2025-01-01 Online:2025-02-28
  • Contact: 茜 王

摘要: 为解决牦牛酥油不易储存,油脂氧化产生的不良风味,本文以麦芽糊精与酪蛋白酸钠作为壁材,分子蒸馏单甘酯、蔗糖酯为乳化剂,瓜尔豆胶为稳定剂包埋牦牛酥油,通过真空冷冻干燥和喷雾干燥的方式制备牦牛酥油微囊粉,对比两者的基本理化性质(水分、溶解度、流变性、表面油、包埋率、得率),微观结构表征及热稳定性。结果表明:两种方式制备的微囊粉为奶白色、无杂质、气味清香。均具有较好的包埋率(94.09%±0.22和92.28%±0.60);冷冻干燥微囊粉(简称冻干粉)的得率98.42%远大于喷雾干燥微囊粉(简称喷干粉)(25.77%),平均颗粒粒径(16.70μm)比喷干粉(24.95μm)小。喷干粉溶解性、流动性优于冻干粉;扫描电镜下微囊粉表面光滑,喷干粉呈圆球形,冻干粉呈不规则形状; 热重分析和差示扫描量热法测定的喷干粉的热稳定性更好。

关键词: 牦牛酥油, 微囊粉, 冷冻干燥, 喷雾干燥, 乳化剂

Abstract: It was dedicated to solve the problem that yak butter is not easy to store and has bad flavor due to fat oxidation, maltodextrin and sodium caseinate were used as wall materials, molecular distillation monoglyceride and sucrose ester were used as emulsifiers, guar gum was used as a stabilizer to encapsulate yak butter, and yak butter microcapsule powder was prepared by vacuum freeze-drying and spray drying methods. The basic physical and chemical properties (moisture content, solubility, rheology, surface oil, encapsulation rate, yield), microscopic structure characterization, and thermal stability of the two were compared. The results showed that the microcapsules prepared by the two methods were milky white, free of impurities and fragrant. Both of them had good embedding rates (94.09%±0.22 and 92.28%±0.60).The yield of freeze-dried microencapsulated powder(98.42%)was significantly higher than that of spray-dried microencapsulated powder(25.77%), and the average particle size(16.70 μm)was smaller than that of spray-dried powder(24.95 μm). The solubility and fluidity of spray-dried powder were superior to those of freeze-dried powder. Under the scanning electron microscope, the surface of microencapsulated powder was smooth, the spray-dried powder was spherical, and the freeze-dried powder was irregular. The thermal stability of the spray-dried powder determined by TGA and differential scanning calorimetry was better.

Key words: yak butter, microencapsulated powder, freeze drying, spray drying, emulsifier